We did an experiment called oxidation of toluene. after refluxing the suspension of toluene in alkaline kmno4, the reaction mixture was treated sequentially with sulfuric acid and oxalic acid to isolate benzoic acid. what was the role of oxalic acid?

The following reaction shows the products when sulfuric acid and aluminum hydroxide react. al(oh)3 + h2so4 → al2(so4)3 + h2o the table shows the calculated amounts of reactants and products when the reaction was conducted in a laboratory. sulfuric acid aluminum hydroxide initial amount of reactant 40 g 15 g theoretical yield of water from reactant 14.69 g 10.38 g what is the approximate amount of the leftover reactant? 11.73 g of sulfuric acid 10.33 g of sulfuric acid 11.12 g of aluminum hydroxide 13.67 g of aluminum hydroxide

Straightforward questions answered in the powerpoint slidesreaction: heating the starting materials under refluxwhat does it mean to heat under reflux? why do we choose water as the reflux solvent? what are boiling chips used for? why do we put a condenser on top of the reaction? why do we add heat and let the reaction stir for 30 minutes? why do we add sulfuric acid to the reaction after it cools as opposed to when it’s still hot? separation: filtration of precipitatewhy don’t we do an aqueous and organic extraction in the separatory funnel? why do you rinse the salicylic acid on the filter with ice cold water? purification: recrystallization of salicylic acid (no hot filtration needed)what is the difference in the amount of room temperature water vs. boiling water needed to dissolve the salicylic acid (assume a 1.2 gram yield of salicylic acid)? remember, in the lab if you need x ml of boiling water to dissolve a solid, then you should add a little more (definitely no more than 1.5 times the theoretical amount) to ensure it doesn’t recrystallize prematurely.analysis: melting point of salicylic acidwhat can you conclude if the melting point of the salicylic acid you just synthesized is 152-155oc and the 1: 1 mix of your product and “synthetic” salicylic acid is 151-154oc?

Is a measure of the resistance to flow. a high liquid has a high resistance to flow and flows slowly. the ancients thought everything in the world was made of 4 we now know that there are 94 naturally occurring and scientists have created another 24 i am certain they will create even more. honey flows slowly because it has a high to flowing. a can be separated by physical means because it contains more than one pure substance and 2 pure substances are not chemically bonded to each other. a cannot be separated by physical means. all matter is made up of all elements are with the same number of protons. if it is just a single or many bonded together, if all of them have the same number of protons, it is an element. in a piece of pure iron metal, all the are joined together, that piece of iron metal is called elemental iron. a single of iron is called elemental iron. a mixture has differences from place to place. we might need a microscope to see them or they might be obvious to the unaided eye. there are surfaces separating it into different phases. a mixture is the same everywhere. it is uniform. there are no surfaces separating it into different phases. if different kinds of atoms (different elements) are bonded together by their electrons, it is called a there are physical means of to isolate the different pure substances in a mixture and there are chemical means of to isolate the different elements in a compound. 1. element 2. compound 3. mixture 4. heterogeneous 5. homogeneous 6. pure substance 7. atoms 8. separation 9. viscosity 10. resistance