In this lab exercise a solution containing K+ is passed down an ion exchange column containing a cation exchange resin in the acid form. The K+ ions in the solution replace the resin bound H3O+ ions which elute from the column and then are titrated. This means that the column now holds the K+ ions. To use the column again we must "recharge" the column to remove K+ ions. In your Lab Notebook, describe the exact procedure you will follow to "recharge" the exchange column for the next use. A 0.171 gram solution of KxFe(C2O4)yzH2O is dissolved in water and the solution is passed down a column containing a cation exchange resin in the acid form. The eluted solution is then titrated with a standard NaOH solution to the first equivalence point. Experimentally it required 11.71 mL of a 0.132 M NaOH solution to reach the first equivalence point. Calculate the number of moles of K+ in the weighted sample.

Your roll: experienced electron speech is adressed to: a new "freshman class" of electrons job: write a speech task: you are to pretend that you are giving a speech to a new group of electrons. be sure to mention their placement in an atom, their charge, and their role in chemical bonding (ionic and covalent) be specific!

0.09 moles of sodium sulfate in 12 ml of solution

Straightforward questions answered in the powerpoint slidesreaction: heating the starting materials under refluxwhat does it mean to heat under reflux? why do we choose water as the reflux solvent? what are boiling chips used for? why do we put a condenser on top of the reaction? why do we add heat and let the reaction stir for 30 minutes? why do we add sulfuric acid to the reaction after it cools as opposed to when it’s still hot? separation: filtration of precipitatewhy don’t we do an aqueous and organic extraction in the separatory funnel? why do you rinse the salicylic acid on the filter with ice cold water? purification: recrystallization of salicylic acid (no hot filtration needed)what is the difference in the amount of room temperature water vs. boiling water needed to dissolve the salicylic acid (assume a 1.2 gram yield of salicylic acid)? remember, in the lab if you need x ml of boiling water to dissolve a solid, then you should add a little more (definitely no more than 1.5 times the theoretical amount) to ensure it doesn’t recrystallize prematurely.analysis: melting point of salicylic acidwhat can you conclude if the melting point of the salicylic acid you just synthesized is 152-155oc and the 1: 1 mix of your product and “synthetic” salicylic acid is 151-154oc?