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Chemistry, 12.10.2020 01:01 jellybellyje

Order the steps required to extract a dichloromethane solution with aqueous hydrochloric acid. Transfer the "Organic Layer" back to the empty separatory funnel.
b. Add an equivalent volume of aqueous acid to the dichloromethane layer in the separatory funnel.
h. Label this beaker "Aqueous Layer".
Remove the cap.
Label the beaker "Organic Layer".
Make sure the stopcock is closed.
Repeat all steps. Drain the bottom layer into a labeled beaker.
C. Cap the separatory funnel with a glass or Teflon stopper.
e. Place the separatory funnel back in the Iron ring.
Remove the funnel from the iron ring and shake vigorously to mix the layers, periodically venting to release pressure. Drain the remaining liquid into a labeled beaker. Suspend a separatory funnel using an iron ring and ring stand. g.
Allow the layers to physically separate in the funnel. Transfer the organic (dichloromethane) layer to the funnel.

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